Cobalt-nickel supported on desilicated HZSM-5 for the conversion of Reutealis trisperma (blanco) airy shaw oil to liquid hydrocarbon products
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Abstract
Desilication/alkaline treatment and metal impregnation were used to create the HZSM-5 catalyst supported by Co-Ni. These catalysts' isotherm patterns combined type I and type IV isotherms. This isotherm pattern showed a hysteresis loop at comparatively higher pressures. The pore size distribution of the mesoporous HZSM-5 catalysts was situated between 6 and 12 nm in size. Its use in the hydrocracking of Reutealis trisperma (Blanco) airy shaw oil (RTO) to produce biofuel was investigated. The results of the catalytic test showed that the hydrocarbon makeup of the biofuel was comparable to that of fuel. In comparison to HZSM-5, the mesoporous Co-Ni/HZSM-5 catalyst enhanced n-paraffin by 46.32 area% and aromatic by 34.18 area% in the hydrocracking of RTO.
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Marlinda, L., Rahmi, Aziz, A., Roesyadi, A., Hari Prajitno, D., & Al-Muttaqii, M. (2025). Cobalt-nickel supported on desilicated HZSM-5 for the conversion of Reutealis trisperma (blanco) airy shaw oil to liquid hydrocarbon products. Communications in Science and Technology, 10(1), 87-97. https://doi.org/10.21924/cst.10.1.2025.1570
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References
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[12] Y. W. Mirzayanti, F. Kurniawansyah, D. Hari Prajitno, and A. Roesyadi, ‘Zn-Mo/HZSM-5 Catalyst for Gasoil Range Hydrocarbon Production by Catalytic Hydrocracking of Ceiba pentandra Oil’, Bulletin of Chemical Reaction Engineering & Catalysis, vol. 13, no. 1, pp. 136–143, 2018, doi: 10.9767/bcrec.13.1.1354.136-143.
[13] L. Qin, J. Li, S. Zhang, Z. Liu, S. Li, and L. Luo, ‘Catalytic performance of Ni-Co/HZSM-5 catalysts for aromatic compound promotion in simulated bio-oil upgrading’, RSC Adv, vol. 13, no. 11, pp. 7694–7702, Mar. 2023, doi: 10.1039/d2ra07706j.
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[15] I. M. S. Anekwe, B. Oboirien, and Y. M. Isa, ‘Performance evaluation of a newly developed transition metal-doped HZSM-5 zeolite catalyst for single-step conversion of C1-C3 alcohols to fuel-range hydrocarbons’, Energy Advances, vol. 3, no. 6, pp. 1314–1328, May 2024, doi: 10.1039/d3ya00460k.
[16] M. Al-Muttaqii, F. Kurniawansyah, D. H. Prajitno, and A. Roesyadi, ‘Hydrocracking of coconut oil over Ni-Fe/HZSM-5 catalyst to produce hydrocarbon biofuel’, Indonesian Journal of Chemistry, vol. 19, no. 2, pp. 319–327, 2019, doi: 10.22146/ijc.33590.
[17] M. Al-Muttaqii, F. Kurniawansyah, D. H. Prajitno, and A. Roesyadi, ‘Bio-kerosene and bio-gasoil from coconut oils via hydrocracking process over Ni-Fe/HZSM-5 catalyst’, Bulletin of Chemical Reaction Engineering and Catalysis, vol. 14, no. 2, pp. 309–319, Aug. 2019, doi: 10.9767/bcrec.14.2.2669.309-319.
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[20] V. Rac, V. Rakíc, Z. Miladinovíc, D. Stoši?, and A. Aurouxc, ‘Influence of the desilication process on the acidity of HZSM-5 zeolite’, Thermochim Acta, vol. 567, pp. 73–78, 2013, doi: 10.1016/j.tca.2013.01.008.
[21] M. Al-Muttaqii et al., ‘Conversion of Sunan Candlenut Oil to Aromatic Hydrocarbons with Hydrocracking Process Over Nano-HZSM-5 Catalyst’, Bulletin of Chemical Reaction Engineering and Catalysis, vol. 19, no. 1, pp. 141–148, 2024, doi: 10.9767/bcrec.20116.
[22] L. Marlinda, M. Al-Muttaqii, I. Gunardi, A. Roesyadi, and D. H. Prajitno, ‘Hydrocracking of Cerbera manghas Oil with Co-Ni/HZSM-5 as Double Promoted Catalyst’, Bulletin of Chemical Reaction Engineering and Catalysis, vol. 12, no. 2, pp. 167–184, 2017, doi: 10.9767/bcrec.12.2.496.167-184.
[23] A. E. Barrón C. et al., ‘Catalytic hydrocracking of vegetable oil for agrofuels production using Ni-Mo, Ni-W, Pt and TFA catalysts supported on SBA-15’, in Catalysis Today, May 2011, pp. 102–110. doi: 10.1016/j.cattod.2011.01.026.
[24] H. Juwono, A. Zakiyah, R. Subagyo, and Y. Kusumawati, ‘Facile Production of Biodiesel from Candlenut Oil (Aleurites moluccana L.) Using Photocatalytic Method by Nano Sized-ZnO Photocatalytic Agent Synthesized via Polyol Method’, Indonesian Journal of Chemistry, vol. 23, no. 5, pp. 1304–1314, 2023, doi: 10.22146/ijc.82895.
[25] L. Marlinda, M. Al-Muttaqii, A. Roesyadi, and D. H. Prajitno, ‘Effect of cobalt supported on the hierarchical Ni/HZSM-5 catalyst in hydrocracking of Sunan candlenut oil (Reutealis trisperma (Blanco) airy shaw)’, in Journal of Physics: Conference Series, Institute of Physics Publishing, Jan. 2020. doi: 10.1088/1742-6596/1442/1/012048.
[26] K. Shimura, T. Miyazawa, T. Hanaoka, and S. Hirata, ‘Fischer-Tropsch synthesis over alumina supported bimetallic Co-Ni catalyst: Effect of impregnation sequence and solution’, J Mol Catal A Chem, vol. 407, pp. 15–24, Jun. 2015, doi: 10.1016/j.molcata.2015.06.013.
[27] D. Dittmann, E. Kaya, and M. Dyballa, ‘Desilicated ZSM-5 Catalysts: Properties and Ethanol to Aromatics (ETA) Performance’, ChemCatChem, vol. 15, no. 20, pp. 1–12, Oct. 2023, doi: 10.1002/cctc.202300716.
[28] Y. Hou et al., ‘The effect of hierarchical single-crystal ZSM-5 zeolites with different Si/Al ratios on its pore structure and catalytic performance’, Front Chem Sci Eng, vol. 15, no. 2, pp. 269–278, Apr. 2021, doi: 10.1007/s11705-020-1948-3.
[29] L. S. Da Silva, C. A. Araki, S. M. P. Marcucci, V. L. dos S. T. Da Silva, and P. A. Arroyo, ‘Desilication of ZSM-5 and ZSM-12 Zeolites With Different Crystal Sizes: Effect on Acidity and Mesoporous Initiation’, Materials Research, vol. 22, no. 2, pp. 1–9, 2019, doi: 10.1590/1980-5373-MR-2018-0872.
[30] Q. Ma, T. Fu, Y. Wang, H. Li, L. Cui, and Z. Li, ‘Development of mesoporous ZSM-5 zeolite with microporosity preservation through induced desilication’, J Mater Sci, vol. 55, no. 26, pp. 11870–11890, Sep. 2020, doi: 10.1007/s10853-020-04855-5.
[31] S. Wang, Q. Yin, J. Guo, B. Ru, and L. Zhu, ‘Improved Fischer-Tropsch synthesis for gasoline over Ru, Ni promoted Co/HZSM-5 catalysts’, Fuel, vol. 108, pp. 597–603, 2013, doi: 10.1016/j.fuel.2013.02.021.
[32] A. N. Aini, M. Al-Muttaqii, A. Roesyadi, and F. Kurniawansyah, ‘Performance of ni-cu/hzsm-5 catalyst in hydrocracking process to produce biofuel from cerbera manghas oil’, in Key Engineering Materials, Trans Tech Publications Ltd, 2021, pp. 149–156. doi: 10.4028/www.scientific.net/KEM.884.149.
[33] E. D. da S. Ferracine, K. T. G. Carvalho, D. S. A. Silva, and E. A. Urquieta-Gonzalez, ‘Carbon-Templated Mesopores in HZSM-5 Zeolites: Effect on Cyclohexane Cracking’, Catal Letters, vol. 150, no. 12, pp. 3481–3494, Dec. 2020, doi: 10.1007/s10562-020-03262-4.
[34] I. Barroso-Martín, D. Ballesteros-Plata, A. Infantes-Molina, M. O. Guerrero-Pérez, J. Santamaría-González, and E. Rodríguez-Castellón, ‘An Overview of Catalysts for the Hydrodeoxygenation Reaction of Model Compounds from Lignocellulosic Biomass’, IET Renewable Power Generation, vol. 16, no. 14, pp. 3009–3022, Oct. 2022, doi: 10.1049/rpg2.12477.
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